1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone

Base Information

• Chemical Name: 1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone
• CAS No.: 82811-25-4
• Molecular Formula: C₁₅H₂₀N₂O₃
• Molecular Weight: 276.335
• Mol file: 82811-25-4.mol

Synonyms:1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone

Chemical Property of 1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone

There total 1 articles about 1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dimethylglyoxal (431-03-8) + N-(2-methyl-1-oximino-1-p-tolyl-2-propyl)hydroxylamine → 1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone (82811-25-4)

Guidance literature:

DOI:10.1007/BF00949952

Reference yield: 98.0%

1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone (82811-25-4) → 4,5,7,7-Tetramethyl-1-p-tolyl-2,3,6,8-tetraaza-bicyclo[3.2.1]oct-3-ene-6,8-diol (82811-33-4)

Guidance literature:

With hydrazine hydrate; In ethanol; for 10h;

DOI:10.1007/BF00949952

Reference yield:

1-(1-Hydroxy-2,5,5-trimethyl-3-oxy-4-p-tolyl-2,5-dihydro-1H-imidazol-2-yl)-ethanone (82811-25-4) → 5,6-dimethyl-3-p-tolyl-1,2,4-triazine 4-oxide

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / hydrazine hydrate / ethanol / 10 h

2: 89 percent / PbO₂ / acetone

With hydrazine hydrate; lead dioxide; In ethanol; acetone;

DOI:10.1007/BF00949952

upstream raw materials:

dimethylglyoxal

Downstream raw materials:

4,5,7,7-Tetramethyl-1-p-tolyl-2,3,6,8-tetraaza-bicyclo[3.2.1]oct-3-ene-6,8-diol