1,1-bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadiene

Base Information

Chemical Name:1,1-bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadiene
CAS No.:268225-69-0
Molecular Formula:C₃₂H₃₂GeN₂O₂
Molecular Weight:549.208
Hs Code.:

Synonyms:1,1-bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadiene

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Technology Process of 1,1-bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadiene

There total 1 articles about 1,1-bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 5725-96-2
N,N-dimethylhydroxylamine

: 16030-09-4
1,1-dichloro-2,3,4,5-tetraphenyl-1-germacyclopenta-2,4-diene

: 268225-69-0
1,1-bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadiene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; pentane; byproducts: LiCl; under N2; n-BuLi in hexane added dropwise to Me2NOH in pentane at -20°C, warmed to room temp., stirred for 1 h, solvent removed in vac., residue suspended in THF, cooled to -196°C, Ge-complex in THF added, stirred at -96°C for 1 h; THF removed under vac., extracted with benzene, filtered, benzene was removed in vacuo; elem. anal.;
DOI:10.1039/a909547k