(S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate

Base Information

Chemical Name:(S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate
CAS No.:914097-62-4
Molecular Formula:C₁₆H₂₂N₂O₂S
Molecular Weight:306.429
Hs Code.:

Synonyms:(S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate

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Chemical Property of (S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate

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Technology Process of (S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate

There total 6 articles about (S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 86953-79-9
tert-butyl pyrrolidine-1-carboxylate

: 103-72-0
phenyl isothiocyanate

: 914097-62-4
(S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate

Guidance literature:: tert-butyl pyrrolidine-1-carboxylate; With sec.-butyllithium; sparteine; at -78 ℃; for 2h; Inert atmosphere;

phenyl isothiocyanate; for 2h; Inert atmosphere;
DOI:10.1002/chem.201504247

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 914097-62-4
(S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / Inert atmosphere; Schlenk technique

2: Inert atmosphere; Schlenk technique

3: Lawessons reagent / toluene / Reflux; Inert atmosphere; Schlenk technique

With Lawessons reagent; triethylamine; In toluene;
DOI:10.1002/chem.201304543

Reference yield:

: (S)-N-(tert-Butoxycarbonyl)proline ethyl carbonate

: 914097-62-4
(S)-2-methyl-2-propanyl 2-(phenylcarbamothioyl)-1-pyrrolidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Inert atmosphere; Schlenk technique

2: Lawessons reagent / toluene / Reflux; Inert atmosphere; Schlenk technique

With Lawessons reagent; In toluene;
DOI:10.1002/chem.201304543