tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate

Base Information

Chemical Name:tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate
CAS No.:1355069-50-9
Molecular Formula:C₃₃H₅₇N₃O₅
Molecular Weight:575.833
Hs Code.:

Synonyms:tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate

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Chemical Property of tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate

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Technology Process of tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate

There total 2 articles about tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 135447-09-5
2-(2-(di-octylamino)-2-oxoethoxy)acetic acid

: 108467-99-8
1-(N-Boc-aminomethyl)-3-(aminomethyl)benzene

: 1355069-50-9
tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/ejoc.201100443

Reference yield:

: 1027755-54-9
2-dioctylcarbamoylmethoxy-N-[3-[(2-dioctyl-carbamoylmethoxy-acetylamino)methyl]benzyl]acetamide

: 1355069-50-9
tert-butyl 3-({2-[2-(dioctylamino)-2-oxoethoxy]acetamido}methyl)benzylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: dodecane; octanol / Irradiation

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dodecane; octanol; dichloromethane;
DOI:10.1002/ejoc.201100443