α-phenyl-α-(β-naphthyl)acetone

Base Information

Chemical Name:α-phenyl-α-(β-naphthyl)acetone
CAS No.:116672-41-4
Molecular Formula:C₁₉H₁₆O
Molecular Weight:260.335
Hs Code.:

Synonyms:α-phenyl-α-(β-naphthyl)acetone

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Chemical Property of α-phenyl-α-(β-naphthyl)acetone

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Technology Process of α-phenyl-α-(β-naphthyl)acetone

There total 2 articles about α-phenyl-α-(β-naphthyl)acetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 673-32-5
1-Phenylprop-1-yne

: 3857-83-8
2-naphthyl triflate

: 2-(naphthalen-2-yl)-1-phenyl-propan-1-one

: 116672-41-4
α-phenyl-α-(β-naphthyl)acetone

Guidance literature:: 1-Phenylprop-1-yne; 2-naphthyl triflate; With morpholine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; C₆₀H₆₆FeN₂P₂; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 80 ℃; for 72h; Inert atmosphere; Glovebox; Sealed tube; Molecular sieve;

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; water; regioselective reaction; Inert atmosphere; Glovebox; Sealed tube; Molecular sieve;
DOI:10.1002/anie.201804955

Reference yield:

: 135-19-3
β-naphthol

: 2-(naphthalen-2-yl)-1-phenyl-propan-1-one

: 116672-41-4
α-phenyl-α-(β-naphthyl)acetone

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / Inert atmosphere

2.1: N-methyl-α-isopropylbenzylamine; C60H66FeN2P2; tris-(dibenzylideneacetone)dipalladium(0); N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 72 h / 80 °C / Inert atmosphere; Glovebox; Sealed tube; Molecular sieve

2.2: Inert atmosphere; Glovebox; Sealed tube; Molecular sieve

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-methyl-α-isopropylbenzylamine; C₆₀H₆₆FeN₂P₂; triethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane;
DOI:10.1002/anie.201804955