2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide

Base Information

Chemical Name:2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide
CAS No.:1386874-78-7
Molecular Formula:C₂₆H₂₀N₆O₃
Molecular Weight:464.483
Hs Code.:

Synonyms:2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide

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Chemical Property of 2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide

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Technology Process of 2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide

There total 4 articles about 2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 14371-10-9
(E)-3-phenylpropenal

: 1386875-02-0
2-((2-(3-nitrophenyl)hydrazinylidene)methyl)quinoline-4-carbohydrazide

: 1386874-78-7
2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide

Guidance literature:: With acetic acid; In ethanol; at 80 ℃; for 2h;
DOI:10.1021/jm300146f

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 1386874-78-7
2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydroxide / water / 0.67 h / 50 °C

1.2: 15 h / 50 °C

1.3: 20 °C / pH 3

2.1: sulfuric acid / 18 h / Reflux

3.1: selenium(IV) oxide / 1,4-dioxane / 4 h / Reflux

4.1: acetic acid / ethanol / 2 h / 80 °C

5.1: hydrazine hydrate / 20 h / 120 °C

6.1: acetic acid / ethanol / 2 h / 80 °C

With selenium(IV) oxide; sulfuric acid; hydrazine hydrate; acetic acid; potassium hydroxide; In 1,4-dioxane; ethanol; water;
DOI:10.1021/jm300146f

Reference yield:

: 634-38-8
2-methylquinoline-4-carboxylic acid

: 1386874-78-7
2-((2-(3-nitrophenyl)hydrazinylidene)methyl)-N'-((E)-3-phenylallylidene)quinoline-4-carbohydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 18 h / Reflux

2: selenium(IV) oxide / 1,4-dioxane / 4 h / Reflux

3: acetic acid / ethanol / 2 h / 80 °C

4: hydrazine hydrate / 20 h / 120 °C

5: acetic acid / ethanol / 2 h / 80 °C

With selenium(IV) oxide; sulfuric acid; hydrazine hydrate; acetic acid; In 1,4-dioxane; ethanol;
DOI:10.1021/jm300146f