phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate

Base Information

• Chemical Name: phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate
• CAS No.: 1017848-87-1
• Molecular Formula: C₂₃H₁₇NO₅
• Molecular Weight: 387.392

Synonyms:phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate

Chemical Property of phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate

There total 2 articles about phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-(4-methoxyphenyl)-4-phenyloxazol-5-yl phenyl carbonate (627877-67-2) → phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate (1017848-87-1)

Guidance literature:

With 3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; In dichloromethane; at 20 - 25 ℃; for 0.25h;

DOI:10.1039/b805850d

Reference yield: 75.0%

2-p-methoxyphenyl-4-phenyl-2-oxazolin-5-one (28172-58-9) + phenyl chloroformate (1885-14-9) → phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate (1017848-87-1)

Guidance literature:

With 2-phenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; triethylamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b806816j

Reference yield:

phenyl 2-(4-methoxyphenyl)-5-oxo-4-phenyl-4,5-dihydrooxazole-4-carboxylate (1017848-87-1) → N-(p-anisoyl)phenylglycine phenyl ester (1017848-94-0)

Guidance literature:

With silica gel; In diethyl ether; Petroleum ether;

DOI:10.1021/jo702720a

upstream raw materials:

2-(4-methoxyphenyl)-4-phenyloxazol-5-yl phenyl carbonate

2-p-methoxyphenyl-4-phenyl-2-oxazolin-5-one

phenyl chloroformate

Downstream raw materials:

N-(p-anisoyl)phenylglycine phenyl ester

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