C₃₂H₆₀O₄Si₂

Base Information

Chemical Name:C₃₂H₆₀O₄Si₂
CAS No.:902131-87-7
Molecular Formula:C₃₂H₆₀O₄Si₂
Molecular Weight:564.997
Hs Code.:

C<sub>32</sub>H<sub>60</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₂H₆₀O₄Si₂

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Chemical Property of C₃₂H₆₀O₄Si₂

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Technology Process of C₃₂H₆₀O₄Si₂

There total 9 articles about C₃₂H₆₀O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 902131-86-6
C₂₆H₄₆O₄Si

: 18162-48-6
tert-butyldimethylsilyl chloride

: 902131-87-7
C₃₂H₆₀O₄Si₂

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 7h;
DOI:10.1039/b602020h

Reference yield:

: 902131-79-7
C₃₃H₃₆O₃

: 902131-87-7
C₃₂H₆₀O₄Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: 90 percent / TsOH*H₂O / methanol / 0.33 h / 25 °C

2.1: 99 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

3.1: 99 percent / MgBr₂ / diethyl ether / 3 h / 0 °C

4.1: 95 percent / imidazole; 4-DMAP / CH₂Cl₂ / 16 h / 20 °C

5.1: BH₃*SMe₂ / tetrahydrofuran / 7 h / 0 - 25 °C

5.2: 85 percent / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

6.1: 93 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

7.1: diethyl ether; tetrahydrofuran / 3 h / -78 °C

7.2: 62.3 g / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

8.1: 89 percent / imidazole; 4-DMAP / CH₂Cl₂ / 7 h / 20 °C

With 1H-imidazole; dmap; oxalyl dichloride; dimethylsulfide borane complex; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 2.1: Swern oxidation / 6.1: Swern oxidation / 7.1: Brown allylation;
DOI:10.1039/b602020h

Reference yield:

: 902131-80-0
C₁₄H₂₂O₃

: 902131-87-7
C₃₂H₆₀O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 99 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

2.1: 99 percent / MgBr₂ / diethyl ether / 3 h / 0 °C

3.1: 95 percent / imidazole; 4-DMAP / CH₂Cl₂ / 16 h / 20 °C

4.1: BH₃*SMe₂ / tetrahydrofuran / 7 h / 0 - 25 °C

4.2: 85 percent / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

5.1: 93 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

6.1: diethyl ether; tetrahydrofuran / 3 h / -78 °C

6.2: 62.3 g / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

7.1: 89 percent / imidazole; 4-DMAP / CH₂Cl₂ / 7 h / 20 °C

With 1H-imidazole; dmap; oxalyl dichloride; dimethylsulfide borane complex; dimethyl sulfoxide; triethylamine; magnesium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Swern oxidation / 5.1: Swern oxidation / 6.1: Brown allylation;
DOI:10.1039/b602020h