Technology Process of C19H19Cl2NO
There total 5 articles about C19H19Cl2NO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
ethanol; water;
at 0 - 20 ℃;
Cooling with ice;
DOI:10.1002/ardp.201200443
- Guidance literature:
-
Multi-step reaction with 4 steps
1: calcium carbonate / water / 7 h / Reflux
2: triethylamine / tetrahydrofuran; dichloromethane / 26 h / 20 °C
3: lithium chloride / N,N-dimethyl-formamide / 0.5 h / 110 °C
4: sodium hydroxide / ethanol; water / 0 - 20 °C / Cooling with ice
With
triethylamine; calcium carbonate; lithium chloride; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
4: |Claisen-Schmidt Condensation;
DOI:10.1002/ardp.201200443
- Guidance literature:
-
Multi-step reaction with 5 steps
1: iron; ammonium chloride; acetic acid / ethanol; water / Reflux
2: calcium carbonate / water / 7 h / Reflux
3: triethylamine / tetrahydrofuran; dichloromethane / 26 h / 20 °C
4: lithium chloride / N,N-dimethyl-formamide / 0.5 h / 110 °C
5: sodium hydroxide / ethanol; water / 0 - 20 °C / Cooling with ice
With
iron; ammonium chloride; acetic acid; triethylamine; calcium carbonate; lithium chloride; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
5: |Claisen-Schmidt Condensation;
DOI:10.1002/ardp.201200443