o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

Base Information

Chemical Name:o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate
CAS No.:104754-68-9
Molecular Formula:C₂₀H₁₈N₂O₈
Molecular Weight:414.372
Hs Code.:

Synonyms:o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

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Chemical Property of o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

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Technology Process of o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

There total 4 articles about o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 104754-51-0
N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylic acid

: 3958-60-9
2-nitrophenylmethyl bromide

: 104754-68-9
o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

Guidance literature:: With triethylamine; In ethyl acetate; for 4h; Heating;
DOI:10.1016/S0040-4020(01)96774-2

Reference yield:

: 328-50-7
α-ketoglutaric acid

: 104754-68-9
o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / 4 h / 80 °C / 10 - 15 Torr

2: 89 percent / Et₃N / ethyl acetate / 4 h / Heating

With triethylamine; In ethyl acetate;
DOI:10.1016/S0040-4020(01)96774-2

Reference yield:

: 621-84-1
O-benzyl carbamate

: 104754-68-9
o-nitrobenzyl N-benzyloxycarbonyl-2-aminotetrahydro-5-oxo-2-furancarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / 4 h / 80 °C / 10 - 15 Torr

2: 89 percent / Et₃N / ethyl acetate / 4 h / Heating

With triethylamine; In ethyl acetate;
DOI:10.1016/S0040-4020(01)96774-2