3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine

Base Information

Chemical Name:3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine
CAS No.:199792-94-4
Molecular Formula:C₄₀H₃₉N₃O₁₁
Molecular Weight:737.763
Hs Code.:

Synonyms:3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine

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Chemical Property of 3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine

Chemical Property:

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Technology Process of 3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine

There total 4 articles about 3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 112141-36-3
5'-O-[2-(4-nitrophenyl)ethoxycarbonyl]thymidine

: 199792-94-4
3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine

Guidance literature:: With pyridine; at 60 ℃; for 4h;
DOI:10.1080/07328319708006249

Reference yield:

: 88091-68-3
2-(4-nitrophenyl)ethoxycarbonyl chloride

: 199792-94-4
3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine

2: 94 percent / pyridine / CH₂Cl₂ / 2 h / 60 °C

With pyridine; In dichloromethane; 1: Condensation / 2: Condensation;
DOI:10.1002/1522-2675(20000809)83:8<2023::AID-HLCA2023>3.0.CO;2-P

Reference yield:

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 199792-94-4
3'-O-(4,4'-dimethoxytrityl)-5'-O-{[2-(4-nitrophenyl)ethoxy]carbonyl}thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine

2: 94 percent / pyridine / CH₂Cl₂ / 2 h / 60 °C

With pyridine; In dichloromethane; 1: Condensation / 2: Condensation;
DOI:10.1002/1522-2675(20000809)83:8<2023::AID-HLCA2023>3.0.CO;2-P