2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

Base Information

Chemical Name:2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol
CAS No.:1312615-97-6
Molecular Formula:C₂₇H₂₈N₆O
Molecular Weight:452.559
Hs Code.:

Synonyms:2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

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Chemical Property of 2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

Chemical Property:

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Technology Process of 2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

There total 7 articles about 2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1154878-10-0
C₁₃H₁₅N₃

: 1312615-95-4
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-phenol

: 1312615-97-6
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

Guidance literature:: C₁₃H₁₅N₃; With hydrogenchloride; sodium nitrite; In methanol; at 0 ℃; for 0.5h;

2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-phenol; With sodium hydroxide; In methanol; at 23 ℃; for 2h;
DOI:10.1002/ejoc.201100216

Reference yield:

: 1312616-01-5
{2-[(pyridin-2-ylmethyl)-amino]-phenyl}carbamic acid benzyl ester

: 1312615-97-6
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; water / 0.5 h / 23 °C

1.2: 24 h / 23 °C

2.1: hydrogenchloride / water / 6 h / 100 °C

3.1: hydrogenchloride; sodium nitrite / methanol / 0.5 h / 0 °C

3.2: 2 h / 23 °C

With hydrogenchloride; sodium nitrite; In methanol; water;
DOI:10.1002/ejoc.201100216

Reference yield:

: 2835-95-2
amino-4 hydroxy-2 toluene

: 1312615-97-6
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 24 h / 23 °C

1.2: 18 h / 23 °C

2.1: sodium cyanoborohydride; acetic acid / water; acetonitrile / 24 h / 23 °C

3.1: hydrogenchloride; sodium nitrite / methanol / 0.5 h / 0 °C

3.2: 2 h / 23 °C

With hydrogenchloride; sodium cyanoborohydride; acetic acid; sodium nitrite; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1002/ejoc.201100216