2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether

Base Information

Chemical Name:2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether
CAS No.:1312615-98-7
Molecular Formula:C₂₈H₃₀N₆O
Molecular Weight:466.586
Hs Code.:

Synonyms:2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether

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Chemical Property of 2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether

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Technology Process of 2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether

There total 10 articles about 2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.1%

: 1312615-97-6
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenol

: 74-88-4
methyl iodide

: 1312615-98-7
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 23 ℃; for 18h;
DOI:10.1002/ejoc.201100216

Reference yield:

: 1154878-10-0
C₁₃H₁₅N₃

: 1312615-98-7
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / methanol / 0.5 h / 0 °C

1.2: 2 h / 23 °C

2.1: potassium hydroxide / dimethyl sulfoxide / 18 h / 23 °C

With hydrogenchloride; potassium hydroxide; sodium nitrite; In methanol; dimethyl sulfoxide;
DOI:10.1002/ejoc.201100216

Reference yield:

: 1312616-01-5
{2-[(pyridin-2-ylmethyl)-amino]-phenyl}carbamic acid benzyl ester

: 1312615-98-7
2-methyl-5-(methyl-pyridin-2-ylmethyl-amino)-4-[2-(methyl-pyridin-2-ylmethyl-amino)-phenylazo]-phenyl methyl ether

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; water / 0.5 h / 23 °C

1.2: 24 h / 23 °C

2.1: hydrogenchloride / water / 6 h / 100 °C

3.1: hydrogenchloride; sodium nitrite / methanol / 0.5 h / 0 °C

3.2: 2 h / 23 °C

4.1: potassium hydroxide / dimethyl sulfoxide / 18 h / 23 °C

With hydrogenchloride; potassium hydroxide; sodium nitrite; In methanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201100216