(4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

Base Information

Chemical Name:(4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride
CAS No.:1582229-74-0
Molecular Formula:C₁₈H₂₃NO₄*ClH
Molecular Weight:353.846
Hs Code.:

Synonyms:(4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

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Chemical Property of (4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

Chemical Property:

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Technology Process of (4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

There total 6 articles about (4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1582229-71-7
1-[azido(3,4-dimethoxyphenyl)methyl]-4,5-dimethoxy-2-methylbenzene

: 1582229-74-0
(4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

Guidance literature:: With chloroform; palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 24h;
DOI:10.3109/14756366.2012.763163

Reference yield:

: 101788-16-3
4,5,3',4'-Tetramethoxy-2-methyl-benzhydrol

: 1582229-74-0
(4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 4 h / 20 °C

2: sodium azide / N,N-dimethyl-formamide / 18 h / 60 - 70 °C

3: palladium on activated charcoal; hydrogen; chloroform / methanol / 24 h / 20 °C

With sodium azide; chloroform; palladium on activated charcoal; hydrogen; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3109/14756366.2012.763163

Reference yield:

: 494-99-5
1,2-dimethoxy-4-methylbenzene

: 1582229-74-0
(4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: polyphosphoric acid / 1 h / 80 °C

2: sodium tetrahydroborate / methanol; tetrahydrofuran / 4.5 h / 0 - 20 °C

3: triethylamine / dichloromethane / 4 h / 20 °C

4: sodium azide / N,N-dimethyl-formamide / 18 h / 60 - 70 °C

5: palladium on activated charcoal; hydrogen; chloroform / methanol / 24 h / 20 °C

With sodium tetrahydroborate; sodium azide; chloroform; palladium on activated charcoal; hydrogen; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3109/14756366.2012.763163