N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide

Base Information

Chemical Name:N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide
CAS No.:1582229-77-3
Molecular Formula:C₁₉H₂₅NO₆S
Molecular Weight:395.477
Hs Code.:

Synonyms:N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide

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Chemical Property of N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide

Chemical Property:

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Technology Process of N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide

There total 7 articles about N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1582229-74-0
(4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride

: 124-63-0
methanesulfonyl chloride

: 1582229-77-3
N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide

Guidance literature:: (4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methanamine hydrochloride; With sodium hydroxide; In methanol; at 20 ℃; for 3h;

methanesulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 20h;
DOI:10.3109/14756366.2012.763163

Reference yield:

: 101788-16-3
4,5,3',4'-Tetramethoxy-2-methyl-benzhydrol

: 1582229-77-3
N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 4 h / 20 °C

2.1: sodium azide / N,N-dimethyl-formamide / 18 h / 60 - 70 °C

3.1: palladium on activated charcoal; hydrogen; chloroform / methanol / 24 h / 20 °C

4.1: sodium hydroxide / methanol / 3 h / 20 °C

4.2: 20 h / 20 °C

With sodium azide; chloroform; palladium on activated charcoal; hydrogen; triethylamine; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3109/14756366.2012.763163

Reference yield:

: 1582229-71-7
1-[azido(3,4-dimethoxyphenyl)methyl]-4,5-dimethoxy-2-methylbenzene

: 1582229-77-3
N-((4,5-dimethoxy-2-methylphenyl)(3,4-dimethoxyphenyl)methyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium on activated charcoal; hydrogen; chloroform / methanol / 24 h / 20 °C

2.1: sodium hydroxide / methanol / 3 h / 20 °C

2.2: 20 h / 20 °C

With chloroform; palladium on activated charcoal; hydrogen; sodium hydroxide; In methanol;
DOI:10.3109/14756366.2012.763163