N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

Base Information

Chemical Name:N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide
CAS No.:1391838-80-4
Molecular Formula:C₂₄H₃₁NO₈S
Molecular Weight:493.578
Hs Code.:

Synonyms:N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

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Chemical Property of N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

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Technology Process of N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

There total 5 articles about N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1391838-77-9
N-(3,6,9,12-tetraoxadodecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

: 98-59-9
p-toluenesulfonyl chloride

: 1391838-80-4
N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1002/chem.201200382

Reference yield:

: 86770-67-4
2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethanol

: 1391838-80-4
N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine / tetrahydrofuran; water / 19 h / 0 - 20 °C

2: pyridine / 2.5 h / Reflux

3: triethylamine / dichloromethane / 24 h / 0 - 20 °C

With pyridine; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201200382

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1391838-80-4
N-(11-(p-tolylsulfonyloxy)-3,6,9-trioxaundecan-1-yl)-exo-norborn-5-en-2,3-dicarboximide

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

2: sodium azide / N,N-dimethyl-formamide / 1.5 h / 60 °C

3: triphenylphosphine / tetrahydrofuran; water / 19 h / 0 - 20 °C

4: pyridine / 2.5 h / Reflux

5: triethylamine / dichloromethane / 24 h / 0 - 20 °C

With pyridine; sodium azide; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201200382