benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

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Chemical Name:benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside
CAS No.:81082-01-1
Molecular Formula:C₃₃H₄₄N₄O₁₁
Molecular Weight:672.733
Hs Code.:

Synonyms:benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

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Chemical Property of benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

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Technology Process of benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

There total 4 articles about benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 69323-70-2,79982-03-9,81131-16-0
benzyl 2-acetamido-2-deoxy-5,6-O-isopropylidene-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

: 81082-01-1
benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

Guidance literature:: With acetic acid; at 40 ℃; for 5h;
DOI:10.1021/jm00351a005

Reference yield:

: 58886-33-2
benzyl 2-acetamido-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

: 81082-01-1
benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) 1,4-dioxane, 95 deg C, 1 h, 2.) 1,4-dioxane, 65 deg C, overnight

2: N-methylmorpholine / dimethylformamide / 0.08 h / -15 °C

3: N-methylmorpholine / dimethylformamide / 4 h / -15 °C

4: 96 percent / 65percent aq. AcOH / 5 h / 40 °C

With 4-methyl-morpholine; sodium hydride; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00351a005

Reference yield:

: C₂₆H₃₇NO₁₀

: 81082-01-1
benzyl 2-acetamido-2-deoxy-3-O-<(R)-2-propionyl-L-alanyl-D-isoglutamine benzyl ester>-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / dimethylformamide / 4 h / -15 °C

2: 96 percent / 65percent aq. AcOH / 5 h / 40 °C

With 4-methyl-morpholine; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00351a005