C₆₈H₉₈N₂O₁₇Si

Base Information

• Chemical Name: C₆₈H₉₈N₂O₁₇Si
• CAS No.: 700377-66-8
• Molecular Formula: C₆₈H₉₈N₂O₁₇Si
• Molecular Weight: 1243.61
• Mol file: 700377-66-8.mol

Synonyms:C₆₈H₉₈N₂O₁₇Si

Chemical Property of C₆₈H₉₈N₂O₁₇Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₈H₉₈N₂O₁₇Si

There total 5 articles about C₆₈H₉₈N₂O₁₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenethyl isocyanate (1943-82-4) + C59H89NO16Si (518980-12-6) → C68H98N2O17Si (700377-66-8)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/jm034233n

Reference yield:

2'-O-acetyltylosin (69988-46-1) → C68H98N2O17Si (700377-66-8)

Guidance literature:

Multi-step reaction with 4 steps

1: p-toluenesulfonic acid monohydrate / benzene / 4 h / Heating

2: acetonitrile / 16 h / 20 °C

3: 1.25 g / imidazole / dimethylformamide / 16 h / 20 °C

4: triethylamine / CH₂Cl₂ / 16 h / 20 °C

With 1H-imidazole; toluene-4-sulfonic acid; triethylamine; acetonitrile; In dichloromethane; N,N-dimethyl-formamide; benzene;

DOI:10.1021/jm034233n

Reference yield:

tylosin (1401-69-0) → C68H98N2O17Si (700377-66-8)

Guidance literature:

Multi-step reaction with 5 steps

1: 100 percent / acetone / 2 h / 20 °C

2: p-toluenesulfonic acid monohydrate / benzene / 4 h / Heating

3: acetonitrile / 16 h / 20 °C

4: 1.25 g / imidazole / dimethylformamide / 16 h / 20 °C

5: triethylamine / CH₂Cl₂ / 16 h / 20 °C

With 1H-imidazole; toluene-4-sulfonic acid; triethylamine; acetonitrile; In dichloromethane; N,N-dimethyl-formamide; acetone; benzene;

DOI:10.1021/jm034233n

upstream raw materials:

phenethyl isocyanate

C₅₉H₈₉NO₁₆Si

2'-O-acetyltylosin

tylosin

Downstream raw materials:

C₅₀H₇₆N₂O₁₆

C₅₂H₈₀N₂O₁₇