C₄₀H₇₅NO₇Si₃

Base Information

Chemical Name:C₄₀H₇₅NO₇Si₃
CAS No.:1254369-15-7
Molecular Formula:C₄₀H₇₅NO₇Si₃
Molecular Weight:766.294
Hs Code.:

C<sub>40</sub>H<sub>75</sub>NO<sub>7</sub>Si<sub>3</sub>

Synonyms:C₄₀H₇₅NO₇Si₃

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Chemical Property of C₄₀H₇₅NO₇Si₃

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Technology Process of C₄₀H₇₅NO₇Si₃

There total 13 articles about C₄₀H₇₅NO₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254369-13-5
C₃₄H₆₁NO₇Si₂

: 69739-34-0
t-butyldimethylsiyl triflate

: 1254369-15-7
C₄₀H₇₅NO₇Si₃

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ml1002184

Reference yield:

: 1330118-88-1
(5R,6R)-5-(2-(benzyloxy)ethyl)-3,3-diethyl-6,11,11,12,12-pentamethyl-4,10-dioxa-3,11-disilatridecan-6-ol

: 1254369-15-7
C₄₀H₇₅NO₇Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethanol

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.2: -78 - 20 °C

4.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

With 2,6-dimethylpyridine; oxalyl dichloride; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.1: Evans aldol reaction;
DOI:10.1021/ml1002184

Reference yield:

: 117643-47-7
C₁₃H₁₈O₂

: 1254369-15-7
C₄₀H₇₅NO₇Si₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene / 36 h / Reflux

2.1: lithium aluminium tetrahydride / diethyl ether / 0.17 h / 0 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / Inert atmosphere

4.1: potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 36 h / 0 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

6.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / ethanol

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: -78 - 20 °C

9.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

10.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; lithium aluminium tetrahydride; oxalyl dichloride; methanesulfonamide; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium carbonate; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium hexacyanoferrate(III); In diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1.1: Johnson-Claisen orthoester rearrangement / 4.1: Sharpless dihydroxylation / 8.1: Swern oxidation / 8.2: Swern oxidation / 9.1: Evans aldol reaction;
DOI:10.1021/ml1002184