1-methylcyclohexyl trichloroacetimidate

Base Information

• Chemical Name: 1-methylcyclohexyl trichloroacetimidate
• CAS No.: 148952-09-4
• Molecular Formula: C₉H₁₄Cl₃NO
• Molecular Weight: 258.575
• Mol file: 148952-09-4.mol

Synonyms:1-methylcyclohexyl trichloroacetimidate

Chemical Property of 1-methylcyclohexyl trichloroacetimidate

Chemical Property:

Purity/Quality:

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Technology Process of 1-methylcyclohexyl trichloroacetimidate

There total 1 articles about 1-methylcyclohexyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Methylcyclohexanol (590-67-0) + trichloroacetonitrile (545-06-2) → 1-methylcyclohexyl trichloroacetimidate (148952-09-4)

Guidance literature:

With potassium hydride; Multistep reaction; 1.) ether, mineral oil, 15 min, 2.) ether, up to r.t.;

DOI:10.1016/S0040-4020(01)86326-2

Reference yield: 35.0%

ethyl 3-hydroperoxy-2-methylenebutanoate (100841-11-0) + 1-methylcyclohexyl trichloroacetimidate (148952-09-4) → ethyl 3-(1-methylcyclohexyl)dioxy-2-methylenebutanoate (188290-44-0)

Guidance literature:

With boron trifluoride diethyl etherate; In Petroleum ether; at -5 ℃; for 0.5h;

DOI:10.1016/S0040-4020(96)01180-5

Reference yield:

tert.-butylhydroperoxide (75-91-2) + 1-methylcyclohexyl trichloroacetimidate (148952-09-4) → tert-butyl-(1-methyl-cyclohexyl)-peroxide (100534-28-9)

Guidance literature:

With boron trifluoride diethyl etherate; In pentane; Yield given; 1.) -5 deg C, 15 min, 2.) up to r.t.;

DOI:10.1016/S0040-4020(01)86326-2

upstream raw materials:

1-Methylcyclohexanol

trichloroacetonitrile

Downstream raw materials:

tert-butyl-(1-methyl-cyclohexyl)-peroxide

ethyl 3-(1-methylcyclohexyl)dioxy-2-methylenebutanoate