4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

Base Information

Chemical Name:4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane
CAS No.:77429-93-7
Molecular Formula:C₅₈H₇₀N₆O₁₀S₄
Molecular Weight:1139.49
Hs Code.:

Synonyms:4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

Suppliers and Price of 4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

There total 7 articles about 4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 77429-96-0
N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

: Methanesulfonic acid 4-[[2-(benzoyl-{2-[(4-methanesulfonyloxy-butyl)-(toluene-4-sulfonyl)-amino]-ethyl}-amino)-ethyl]-(toluene-4-sulfonyl)-amino]-butyl ester

: 77429-93-7
4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 2h;
DOI:10.1021/ja00369a053

Reference yield: 20.0%

: 4724-56-5
1,4-ditosyloxybutane

: 77429-96-0
N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

: 77429-91-5
4-benzoyl-1,7-bis(p-tolylsulfonyl)-1,4,7-triazacycloundecane

: 77429-93-7
4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

Guidance literature:: In N,N-dimethyl-formamide; at 95 ℃; for 2h;
DOI:10.1021/jo00342a006

Reference yield:

: 3634-89-7
N-(p-toluenesulfonyl)aziridine

: 77429-93-7
4,15-dibenzoyl-1,7,12,18-tetrakis(p-tolylsulfonyl)-1,4,7,12,15,18-hexaazacyclodocosane

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / acetonitrile / Heating

2: 80 percent / triethylamine / benzene / temp. below 50 deg C, overnight

3: 95 percent / C₂H₅ONa / ethanol

4: 20 percent / dimethylformamide / 2 h / 95 °C

With sodium ethanolate; triethylamine; In ethanol; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1021/jo00342a006