N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

Base Information

Chemical Name:N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt
CAS No.:77429-96-0
Molecular Formula:C₂₅H₂₇N₃O₅S₂*2Na
Molecular Weight:559.618
Hs Code.:

Synonyms:N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

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Chemical Property of N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

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Technology Process of N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

There total 5 articles about N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 77429-98-2
3-benzoyl-N¹,N⁵-ditosyl-3-azapentane-1,5-diamine

: 77429-96-0
N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

Guidance literature:: With sodium ethanolate; In ethanol;
DOI:10.1021/jo00342a006

Reference yield:

: 3634-89-7
N-(p-toluenesulfonyl)aziridine

: 77429-96-0
N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / acetonitrile / Heating

2: 80 percent / triethylamine / benzene / temp. below 50 deg C, overnight

3: 95 percent / C₂H₅ONa / ethanol

With sodium ethanolate; triethylamine; In ethanol; acetonitrile; benzene;
DOI:10.1021/jo00342a006

Reference yield:

: 6367-75-5
2-(tosylamino)ethyl p-toluenesulfonate

: 77429-96-0
N'-benzoyl-N,N-bis(p-tolylsulfonyl)diethylenetriamine N,N-disodium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / 20percent aq. KOH / benzene / 0.5 h

2: 77 percent / acetonitrile / Heating

3: 80 percent / triethylamine / benzene / temp. below 50 deg C, overnight

4: 95 percent / C₂H₅ONa / ethanol

With potassium hydroxide; sodium ethanolate; triethylamine; In ethanol; acetonitrile; benzene;
DOI:10.1021/jo00342a006