N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

Base Information

Chemical Name:N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine
CAS No.:1533424-29-1
Molecular Formula:C₉H₆BrClF₃N₅
Molecular Weight:356.532
Hs Code.:

N<SUP>3</SUP>-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

Synonyms:N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

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Technology Process of N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

There total 4 articles about N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1533434-96-6
(Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate

: 1533424-29-1
N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

Guidance literature:: With hydrazine; In ethanol; at 70 ℃; for 3h; under 760.051 Torr; Inert atmosphere;

Reference yield: 81.0%

: (Z)-methyl N-4-bromo-3-chloro-5-(trifluoromethyl)phenyl-N'-cyanocarbamimidothioate

: 1533424-29-1
N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

Guidance literature:: With hydrazine; In ethanol; at 70 ℃; for 3h; Inert atmosphere;

Reference yield:

: 914225-58-4
4-bromo-3-chloro-5-(trifluoromethyl)aniline

: 1533424-29-1
N³-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-1H-1,2,4-triazole-3,5-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 0 - 20 °C / 760.05 Torr / Inert atmosphere

2.1: methanol; 1,2-dimethoxyethane / 1.5 h / 20 °C / 760.05 Torr / Inert atmosphere

2.2: 2 h / 20 °C / 760.05 Torr / Inert atmosphere

3.1: hydrazine / ethanol / 3 h / 70 °C / 760.05 Torr / Inert atmosphere

With hydrazine; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane;