(Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate

Base Information

Chemical Name:(Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate
CAS No.:1533434-96-6
Molecular Formula:C₁₀H₆BrClF₃N₃S
Molecular Weight:372.596
Hs Code.:

Synonyms:(Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate

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Chemical Property of (Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate

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Technology Process of (Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate

There total 2 articles about (Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1533425-20-5
2-bromo-1-chloro-5-isothiocyanato-3-(trifluoromethyl)benzene

: 19981-17-0,20611-81-8,123092-13-7,17292-62-5
sodium cyanamide

: 74-88-4
methyl iodide

: 1533434-96-6
(Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate

Guidance literature:: 2-bromo-1-chloro-5-isothiocyanato-3-(trifluoromethyl)benzene; sodium cyanamide; In methanol; 1,2-dimethoxyethane; for 0.5h; under 760.051 Torr; Inert atmosphere;

methyl iodide; In methanol; 1,2-dimethoxyethane; at 20 ℃; Inert atmosphere;

Reference yield:

: 914225-58-4
4-bromo-3-chloro-5-(trifluoromethyl)aniline

: 1533434-96-6
(Z)-methyl N-(4-bromo-3-chloro-5-(trifluoromethyl)phenyl)-N'-cyanocarbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 0 - 20 °C / 760.05 Torr / Inert atmosphere

2.1: methanol; 1,2-dimethoxyethane / 1.5 h / 20 °C / 760.05 Torr / Inert atmosphere

2.2: 2 h / 20 °C / 760.05 Torr / Inert atmosphere

In methanol; 1,2-dimethoxyethane; dichloromethane;