(-)-chloromenthyloxydiphenylsilane

Base Information

• Chemical Name: (-)-chloromenthyloxydiphenylsilane
• CAS No.: 67131-32-2
• Molecular Formula: C₂₂H₂₉ClOSi
• Molecular Weight: 373.01

Synonyms:(-)-chloromenthyloxydiphenylsilane

Chemical Property of (-)-chloromenthyloxydiphenylsilane

Chemical Property:

Purity/Quality:

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Technology Process of (-)-chloromenthyloxydiphenylsilane

There total 1 articles about (-)-chloromenthyloxydiphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

(-)-menthol (2216-51-5) + diphenylsilyl dichloride (80-10-4) → (-)-chloromenthyloxydiphenylsilane (67131-32-2)

Guidance literature:

With triethylamine; In dichloromethane; at 42 ℃; for 72h;

DOI:10.1021/ol049233b

Reference yield: 80.0%

(-)-chloromenthyloxydiphenylsilane (67131-32-2) + (17R)-hydroxyoctadeca-9(Z),12(Z),15(Z)-trienoic acid methyl ester (290307-73-2) → (9Z,12Z,15Z)-(R)-17-[((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-diphenyl-silanyloxy]-octadeca-9,12,15-trienoic acid methyl ester

Guidance literature:

DOI:10.1021/ol006162h

Reference yield: 75.0%

(-)-chloromenthyloxydiphenylsilane (67131-32-2) + (11R,9Z,12Z,15Z)-11-hydroxyoctadeca-9,12,15-trienoic acid methyl ester (290349-14-3) → (9Z,12Z,15Z)-(R)-11-[((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-diphenyl-silanyloxy]-octadeca-9,12,15-trienoic acid methyl ester

Guidance literature:

With dmap; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ol006162h

upstream raw materials:

(-)-menthol

diphenylsilyl dichloride

Downstream raw materials:

C₆₀H₅₈Br₂O₂S₇Si₂

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