1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine

Base Information

• Chemical Name: 1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine
• CAS No.: 426820-07-7
• Molecular Formula: C₄₅H₆₀N₂O₂S
• Molecular Weight: 693.05
• Mol file: 426820-07-7.mol

Synonyms:1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine

Chemical Property of 1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine

There total 5 articles about 1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-isopropylbenzenesulfonyl chloride (54997-90-9) + 1-triphenylmethyl-3-n-tridecylpiperazine (187228-89-3) → 1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine (426820-07-7)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1016/S0223-5234(01)01274-0

Reference yield:

Isopropylbenzene (98-82-8) → 1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine (426820-07-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 82.5 percent / conc. H₂SO₄ / 3 h / 160 °C

2: 60 percent / PCl₅ / CH₂Cl₂ / 3 h / 0 °C

3: triethylamine / CH₂Cl₂ / 3 h / 20 °C

With phosphorus pentachloride; sulfuric acid; triethylamine; In dichloromethane;

DOI:10.1016/S0223-5234(01)01274-0

Reference yield:

p-cumenesulfonic acid (16066-35-6) → 1-(4-isopropyl-benzenesulfonyl)-2-tridecyl-4-trityl-piperazine (426820-07-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / PCl₅ / CH₂Cl₂ / 3 h / 0 °C

2: triethylamine / CH₂Cl₂ / 3 h / 20 °C

With phosphorus pentachloride; triethylamine; In dichloromethane;

DOI:10.1016/S0223-5234(01)01274-0

upstream raw materials:

4-isopropylbenzenesulfonyl chloride

1-triphenylmethyl-3-n-tridecylpiperazine

Isopropylbenzene

p-cumenesulfonic acid