(R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester

Base Information

• Chemical Name: (R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester
• CAS No.: 199847-19-3
• Molecular Formula: C₁₉H₂₄O₂SSi
• Molecular Weight: 344.55

Synonyms:(R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester

Chemical Property of (R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester

There total 2 articles about (R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(Trimethylsilyl)benzenethiol (33356-45-5) + Methyl cinnamate (103-26-4,1754-62-7) → (R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester (199847-19-3) + (S)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester

Guidance literature:

With 2-TMSC₆H₄SLi; (-)-(1R,2R)-1-dimethylamino-2-(2-methoxyphenoxy)-1,2-diphenylethane; In hexane; toluene; at -40 ℃; for 72h; Title compound not separated from byproducts;

DOI:10.1021/ja9729950

Reference yield:

2-(Trimethylsilyl)benzenethiol (33356-45-5) + methyl cinnamate (103-26-4,1754-62-7) → (R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester (199847-19-3)

Guidance literature:

With chiral amino ether-lithium thiolate;

DOI:10.1021/jo015879v

Reference yield:

(R)-3-Phenyl-3-(2-trimethylsilanyl-phenylsulfanyl)-propionic acid methyl ester (199847-19-3) → 3-(2-trimethylsilylphenylsulfanyl)-3-phenylpropanal (392667-96-8)

Guidance literature:

With diisobutylaluminium hydride; In toluene; at -78 ℃; for 0.5h;

DOI:10.1021/jo015879v

upstream raw materials:

2-(Trimethylsilyl)benzenethiol

Methyl cinnamate

methyl cinnamate

Downstream raw materials:

3-(2-trimethylsilylphenylsulfanyl)-3-phenylpropanal

(+)-(R)-methyl 3-phenyl-3-phenylsulfanylpropanoate

(R)-(+)-ethyl-3-phenylsulfanyl-3-phenylpropionate

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