C₁₆H₂₂BrF₂N₃O₂

Base Information

Chemical Name:C₁₆H₂₂BrF₂N₃O₂
CAS No.:1383485-60-6
Molecular Formula:C₁₆H₂₂BrF₂N₃O₂
Molecular Weight:406.27
Hs Code.:

C<sub>16</sub>H<sub>22</sub>BrF<sub>2</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₆H₂₂BrF₂N₃O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₂BrF₂N₃O₂

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Technology Process of C₁₆H₂₂BrF₂N₃O₂

There total 7 articles about C₁₆H₂₂BrF₂N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1259278-17-5,1788036-28-1,609788-04-7,849616-22-4
tert-butyl N-[(1R,3S)-3-aminocyclohexyl]carbamate

: 1186194-66-0
2-bromo-3,5,6-trifluoropyridine

: 1383485-60-6
C₁₆H₂₂BrF₂N₃O₂

Guidance literature:: With triethylamine; In tetrahydrofuran; methanol; at 80 ℃; for 17h;

Reference yield:

: 227783-08-6
(1S,3R)-3-ethoxycarbonylcyclohexane-1-carboxylic acid

: 1383485-60-6
C₁₆H₂₂BrF₂N₃O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / 110 °C

1.2: 70 - 85 °C

2.1: water; lithium hydroxide / tetrahydrofuran

2.2: pH 3

3.1: pyridine; di-tert-butyl dicarbonate; ammonium bicarbonate / 1,4-dioxane

3.2: 1 h

4.1: bis-[(trifluoroacetoxy)iodo]benzene / water; acetonitrile / 20 °C

5.1: potassium carbonate / tetrahydrofuran / 20 °C

6.1: hydrogen / palladium 10% on activated carbon / methanol / 750.08 Torr / Inert atmosphere

7.1: triethylamine / tetrahydrofuran; methanol / 17 h / 80 °C

With pyridine; di-tert-butyl dicarbonate; diphenyl phosphoryl azide; water; hydrogen; ammonium bicarbonate; potassium carbonate; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; lithium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; water; toluene; acetonitrile;

Reference yield:

: 952616-39-6
(1R,3S)-3-(((benzyloxy)carbonyl)amino)cyclohexanecarboxylic acid

: 1383485-60-6
C₁₆H₂₂BrF₂N₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; di-tert-butyl dicarbonate; ammonium bicarbonate / 1,4-dioxane

1.2: 1 h

2.1: bis-[(trifluoroacetoxy)iodo]benzene / water; acetonitrile / 20 °C

3.1: potassium carbonate / tetrahydrofuran / 20 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 750.08 Torr / Inert atmosphere

5.1: triethylamine / tetrahydrofuran; methanol / 17 h / 80 °C

With pyridine; di-tert-butyl dicarbonate; hydrogen; ammonium bicarbonate; potassium carbonate; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; water; acetonitrile;