2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline

Base Information

Chemical Name:2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline
CAS No.:1221497-75-1
Molecular Formula:C₂₀H₁₅FN₂
Molecular Weight:302.351
Hs Code.:

Synonyms:2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline

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Chemical Property of 2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline

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Technology Process of 2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline

There total 2 articles about 2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 3931-87-1
(cyclopent-1-en-1-yloxy)triethylsilane

: 1112200-15-3
C₂₂H₁₇FN₂O₂S

: 1221497-75-1
2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline

Guidance literature:: C₂₂H₁₇FN₂O₂S; With silver trifluoromethanesulfonate; In acetonitrile; at 70 ℃; for 1h;

(cyclopent-1-en-1-yloxy)triethylsilane; With sodium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃;
DOI:10.1021/cc1000314

Reference yield: 68.0%

: 943835-77-6
5-fluoro-2-(2-phenylethynyl)benzaldehyde

: 120-92-3
cyclopentanone

: 1221497-75-1
2-fluoro-6-phenyl-10,11-dihydro-9H-cyclopenta[3,4]pyrazolo[5,1-a]isoquinoline

Guidance literature:: 5-fluoro-2-(2-phenylethynyl)benzaldehyde; With toluene-4-sulfonic acid hydrazide; In ethanol; at 20 ℃; for 0.166667h; Inert atmosphere;

cyclopentanone; With phosphate potassium salt; silver trifluoromethanesulfonate; In ethanol; at 20 - 70 ℃; Inert atmosphere;
DOI:10.1002/adsc.201000176