2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol

Base Information

• Chemical Name: 2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol
• CAS No.: 885069-30-7
• Molecular Formula: C₁₅H₂₂BClO₃
• Molecular Weight: 296.602
• Hs Code.: 2906290090

Synonyms:2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol

Chemical Property of 2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol

Chemical Property:

• Boiling Point: 402.0±40.0 °C(Predicted)
• Density: 1.12±0.1 g/cm3(Predicted)

Purity/Quality:

98%+ ^*data from raw suppliers

2-[2-Chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol ^*data from reagent suppliers

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Technology Process of 2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol

There total 1 articles about 2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(5-bromo-2-chlorophenyl)-1-methylethanol (885069-29-4) + bis(pinacol)diborane (73183-34-3) → 2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol (885069-30-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; In N,N-dimethyl-formamide; at 60 ℃; for 12h;

Reference yield:

2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol (885069-30-7) + 4-chloro-N-{2-[4-(difluoromethoxy)phenyl]ethyl}-6-methoxy-1,3,5-triazin-2-amine (1443151-81-2) → 2-{2-chloro-5-[4-({2-[4-(difluoromethoxy)phenyl]ethyl}amino)-6-methoxy-1,3,5-triazin-2-yl]phenyl}propan-2-ol (1443151-54-9)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,2-dimethoxyethane; water; at 20 ℃; for 48h;

Reference yield:

C12H13ClN4O2 (1406298-76-7) + 2-[2-chloro-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]propan-2-ol (885069-30-7) → 4-[2-({4-[4-Chloro-3-(1-hydroxy-1-methylethyl)phenyl]-6-methoxy-1,3,5-triazin-2-yl}amino)ethyl]phenol (1443151-98-1)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,2-dimethoxyethane; water; for 2.5h; Reflux;

upstream raw materials:

1-(5-bromo-2-chlorophenyl)-1-methylethanol

bis(pinacol)diborane

Downstream raw materials:

2-{2-chloro-5-[4-({2-[4-(difluoromethoxy)phenyl]ethyl}amino)-6-methoxy-1,3,5-triazin-2-yl]phenyl}propan-2-ol

2-{2-chloro-5-[4-( {2-[4-(fluoromethoxy)phenyl]ethyl}amino)-6-methoxy-1,3,5-triazin-2-yl]phenyl}propan-2-ol

4-[2-({4-[4-Chloro-3-(1-hydroxy-1-methylethyl)phenyl]-6-methoxy-1,3,5-triazin-2-yl}amino)ethyl]phenol

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