Technology Process of (RS)-(1l,2l,3u,4l)-2,3-Epoxy-4-pentylcyclohexanol
There total 1 articles about (RS)-(1l,2l,3u,4l)-2,3-Epoxy-4-pentylcyclohexanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium;
In
benzene;
at 40 ℃;
for 48h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 92 percent / CrO3, pyridine / CH2Cl2 / 0.25 h / Ambient temperature
2: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature
3: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux
4: 58 percent / 1 h / 200 °C
5: 94 percent / H2 / Pt-oxide / acetic acid / 1 h
6: 62 percent / K2CO3 / 16 h / Ambient temperature
7: 6 h / 60 °C
With
pyridine; chromium(VI) oxide; mercury(II) diacetate; hydrogen; potassium carbonate; hydrazine hydrate; acetic acid;
Pt-oxide;
In
ethanol; dichloromethane; acetic acid;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 92 percent / CrO3, pyridine / CH2Cl2 / 0.25 h / Ambient temperature
2: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature
3: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux
4: 58 percent / 1 h / 200 °C
5: 94 percent / H2 / Pt-oxide / acetic acid / 1 h
With
pyridine; chromium(VI) oxide; mercury(II) diacetate; hydrogen; hydrazine hydrate; acetic acid;
Pt-oxide;
In
ethanol; dichloromethane; acetic acid;
