Cyclohexaneacetaldehyde, a-(3-oxobutyl)-4-pentyl-

Base Information

Chemical Name:Cyclohexaneacetaldehyde, a-(3-oxobutyl)-4-pentyl-
CAS No.:110568-37-1
Molecular Formula:C₁₇H₃₀O₂
Molecular Weight:266.424
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexaneacetaldehyde, a-(3-oxobutyl)-4-pentyl-

Chemical Property:

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Technology Process of Cyclohexaneacetaldehyde, a-(3-oxobutyl)-4-pentyl-

There total 11 articles about Cyclohexaneacetaldehyde, a-(3-oxobutyl)-4-pentyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98789-91-4
4-n-pentyl-2-cyclohexen-1-one

: 110568-37-1
5-Oxo-2-(4-pentyl-cyclohexyl)-hexanal

Guidance literature:: Multi-step reaction with 9 steps

1: 67 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

2: 53 percent / VO(acac)2, tert-butylhydroperoxide / benzene / 48 h / 40 °C

3: 92 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h / Ambient temperature

4: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature

5: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux

6: 58 percent / 1 h / 200 °C

7: 94 percent / H₂ / Pt-oxide / acetic acid / 1 h

8: 62 percent / K₂CO₃ / 16 h / Ambient temperature

9: 6 h / 60 °C

With pyridine; chromium(VI) oxide; tert.-butylhydroperoxide; lithium aluminium tetrahydride; bis(acetylacetonate)oxovanadium; mercury(II) diacetate; hydrogen; potassium carbonate; hydrazine hydrate; acetic acid; Pt-oxide; In diethyl ether; ethanol; dichloromethane; acetic acid; benzene;

Reference yield:

: 110568-30-4
(RS)-(1l,2l,3u,4l)-2,3-Epoxy-4-pentylcyclohexanol

: 110568-37-1
5-Oxo-2-(4-pentyl-cyclohexyl)-hexanal

Guidance literature:: Multi-step reaction with 7 steps

1: 92 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature

3: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux

4: 58 percent / 1 h / 200 °C

5: 94 percent / H₂ / Pt-oxide / acetic acid / 1 h

6: 62 percent / K₂CO₃ / 16 h / Ambient temperature

7: 6 h / 60 °C

With pyridine; chromium(VI) oxide; mercury(II) diacetate; hydrogen; potassium carbonate; hydrazine hydrate; acetic acid; Pt-oxide; In ethanol; dichloromethane; acetic acid;

Reference yield:

: 110568-31-5
(RS)-(2l,3l,4u)-2,3-Epoxy-4-pentylcyclohexanon

: 110568-37-1
5-Oxo-2-(4-pentyl-cyclohexyl)-hexanal

Guidance literature:: Multi-step reaction with 6 steps

1: 60 percent / hydrazine hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature

2: 85 percent / Hg(II)-acetate / 1) 75 deg , 2 h; 2) 1 h, reflux

3: 58 percent / 1 h / 200 °C

4: 94 percent / H₂ / Pt-oxide / acetic acid / 1 h

5: 62 percent / K₂CO₃ / 16 h / Ambient temperature

6: 6 h / 60 °C

With mercury(II) diacetate; hydrogen; potassium carbonate; hydrazine hydrate; acetic acid; Pt-oxide; In ethanol; acetic acid;