2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide

Base Information

Chemical Name:2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide
CAS No.:332037-96-4
Molecular Formula:C₁₇H₁₄Cl₄N₂O₄
Molecular Weight:452.121
Hs Code.:

Synonyms:2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide

Chemical Property:

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Technology Process of 2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide

There total 5 articles about 2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 58048-37-6
2-(2,4-dichloro-phenoxy)-propionyl chloride

: 28236-62-6
2,4-dichlorophenoxyacetylhydrazine

: 332037-96-4
2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide

Guidance literature:: In tetrahydrofuran; for 0.166667h; Time; Reagent/catalyst; Temperature; Microwave irradiation;
DOI:10.3390/molecules181214876

Reference yield:

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 332037-96-4
2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide / N,N-dimethyl-formamide / 0.07 h / Microwave irradiation

2: hydrazine hydrate / ethanol / 0.02 h / Microwave irradiation

3: tetrahydrofuran / 0.17 h / Microwave irradiation

With tetrabutylammomium bromide; hydrazine hydrate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1111/j.1747-0285.2011.01205.x

Reference yield:

: 533-23-3
ethyl 2,4-dichlorophenoxyacetate

: 332037-96-4
2-(2,4-dichlorophenoxy)-N'-(2-(2,4-dichlorophenoxy)acetyl)propanehydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol; N,N-dimethyl-formamide / 0.03 h / Microwave irradiation

2: tetrahydrofuran / 0.17 h / Microwave irradiation

With hydrazine hydrate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.3390/molecules181214876