2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline

Base Information

Chemical Name:2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline
CAS No.:1262284-78-5
Molecular Formula:C₂₄H₂₀N₄Si
Molecular Weight:392.535
Hs Code.:

Synonyms:2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline

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Technology Process of 2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline

There total 5 articles about 2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 27318-90-7
1,10-phenanthroline-5,6-dione

: 77123-57-0
4-[(trimethylsilyl)ethynyl]bezaldehyde

: 1262284-78-5
2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline

Guidance literature:: With ammonium acetate; acetic acid; for 4h; Reflux; Inert atmosphere;
DOI:10.1021/ic1002868

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 614717-89-4
2-(4-bromophenyl)-1H-imidazo(4,5-f)[1,10]phenanthroline

: 1262284-78-5
2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline

Guidance literature:: With palladium on activated charcoal; triethylamine; In acetonitrile; at 140 ℃; for 0.5h; Microwave irradiation; Inert atmosphere; Sealed tube;

Reference yield:

: 66-71-7
1,10-Phenanthroline

: 1262284-78-5
2-{4-[2-(trimethylsilyl)ethynyl]phenyl}-1H-imidazo[4,5-f ][1,10]phenanthroline

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; nitric acid; potassium bromide / 0 - 100 °C

2: ammonium acetate; acetic acid / 2 h / 70 - 80 °C

With sulfuric acid; ammonium acetate; nitric acid; acetic acid; potassium bromide;
DOI:10.1016/j.bmcl.2011.06.051