(R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

Base Information

Chemical Name:(R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol
CAS No.:289473-21-8
Molecular Formula:C₃₂H₃₆O₂S
Molecular Weight:484.703
Hs Code.:

(R<sub>S</sub>,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

Synonyms:(R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

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Chemical Property of (R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

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Technology Process of (R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

There total 4 articles about (R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: phenylmagnesium bromide

: 289473-20-7
(R_S)-1-[(2,4,6-triisopropyl)sulfinyl]-2-naphthaldehyde

: 289473-21-8
(R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

Guidance literature:: In tetrahydrofuran; at -78 ℃;
DOI:10.1021/jo005581p

Reference yield:

: 103668-59-3
1-bromo-2-naphthaldehyde dimethyl acetal

: 289473-21-8
(R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / n-BuLi / diethyl ether / -105 °C

2: 100 percent / aq. H₂SO₄; SiO₂ / CH₂Cl₂ / 1 h / 20 °C

3: 96 percent / tetrahydrofuran / -78 °C

With n-butyllithium; sulfuric acid; silica gel; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo005581p

Reference yield:

: 320589-32-0
(R)-1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthaldehyde dimethyl acetal

: 289473-21-8
(R_S,S)-1-phenyl-1-[1-[(2,4,6-triisopropylphenyl)sulfinyl]-2-naphthyl]methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / aq. H₂SO₄; SiO₂ / CH₂Cl₂ / 1 h / 20 °C

2: 96 percent / tetrahydrofuran / -78 °C

With sulfuric acid; silica gel; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo005581p