phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate

Base Information

Chemical Name:phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate
CAS No.:98761-71-8
Molecular Formula:C₁₈H₂₃NO₂
Molecular Weight:285.386
Hs Code.:

Synonyms:phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate

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Chemical Property of phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate

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Technology Process of phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate

There total 4 articles about phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5057-12-5
3,4,7,8-tetrahydro-2,5(1H,6H)-quinolinequinone

: 98761-71-8
phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 10percent aq. KOH, H₂ / 10percent Pd/C / methanol / 2 h / 2068.6 Torr / Ambient temperature

2: 1.) n-BuLi / 1.) THF, RT, 4 h, 2.) THF, reflux, 3 h

3: LiAlH₄ / tetrahydrofuran / 5 h / Heating

4: 10percent aq. KOH / tetrahydrofuran / 1 h

With potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm00151a001

Reference yield:

: 98761-70-7
trans-octahydro-5-methylene-2(1H)-quinolinone

: 98761-71-8
phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 5 h / Heating

2: 10percent aq. KOH / tetrahydrofuran / 1 h

With potassium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jm00151a001

Reference yield:

: 70075-68-2
trans-hexahydro-2,5(1H,3H)-quinolinedione

: 98761-71-8
phenylmethyl trans-octahydro-5-methylene-1(2H)quinolinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, RT, 4 h, 2.) THF, reflux, 3 h

2: LiAlH₄ / tetrahydrofuran / 5 h / Heating

3: 10percent aq. KOH / tetrahydrofuran / 1 h

With potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran;
DOI:10.1021/jm00151a001