N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide
• CAS No.: 1286216-04-3
• Molecular Formula: C₅₄H₅₈N₆O₁₀S
• Molecular Weight: 983.155

Synonyms:N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide

Chemical Property of N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide

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Technology Process of N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide

There total 1 articles about N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine (1048636-38-9) + N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-(3-bromopropyl)-4-nitrobenzenesulfonamide (1286216-00-9) → N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide (1286216-04-3)

Guidance literature:

With potassium carbonate; In acetonitrile; for 48h; Reflux;

DOI:10.1055/s-0030-1258337

Reference yield: 78.0%

N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide (1286216-04-3) → N,N,N'-tris{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}propane-1,3-diamine (1286216-08-7)

Guidance literature:

With mercaptoacetic acid; lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1055/s-0030-1258337

upstream raw materials:

N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine

N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-(3-bromopropyl)-4-nitrobenzenesulfonamide

Downstream raw materials:

N,N,N'-tris{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}propane-1,3-diamine

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