N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine

Base Information

• Chemical Name: N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine
• CAS No.: 1048636-38-9
• Molecular Formula: C₃₀H₃₃N₃O₄
• Molecular Weight: 499.61
• Mol file: 1048636-38-9.mol

Synonyms:N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine

Chemical Property of N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine

There total 2 articles about N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-4-nitrobenzenesulfonamide (1286215-86-8) → N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine (1048636-38-9)

Guidance literature:

With mercaptoacetic acid; lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5.5h;

DOI:10.1055/s-0030-1258337

Reference yield:

3-(benzyloxy)-1-(3-chloropropyl)pyridin-2(1H)-one (1048636-37-8) → N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine (1048636-38-9)

Guidance literature:

With ammonia; In methanol; at 130 ℃; for 2h; Microwave irradiation;

Reference yield: 72.0%

N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine (1048636-38-9) + CH3O3S(1-)*C16H18NO(1+) → tris{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine (1286215-93-7)

Guidance literature:

N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine; CH₃O₃S^(1-)*C₁₆H₁₈NO⁽¹⁺⁾; With triethylamine; In acetonitrile; at 60 ℃; for 22h;

In acetonitrile;

DOI:10.1055/s-0030-1258337

upstream raw materials:

3-(benzyloxy)-1-(3-chloropropyl)pyridin-2(1H)-one

N,N-bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-4-nitrobenzenesulfonamide

Downstream raw materials:

2,2'-(4,4'-(5-(bis(3-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)propyl)amino)-5-oxopentane-2,2-diyl)bis(4,1-phenylene))bis(oxy)bis(ethane-2,1-diyl)bis(2-methylacrylate)

N-{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}-N-[3-(bis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amino)propyl]-4-nitrobenzenesulfonamide

tris{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}amine

N,N,N',N'-tetrakis{3-[3-(benzyloxy)-2-oxopyridin-1(2H)-yl]propyl}propane-1,3-diamine