C₃₇H₄₃IO₈

Base Information

Chemical Name:C₃₇H₄₃IO₈
CAS No.:374752-89-3
Molecular Formula:C₃₇H₄₃IO₈
Molecular Weight:742.648
Hs Code.:

C<sub>37</sub>H<sub>43</sub>IO<sub>8</sub>

Synonyms:C₃₇H₄₃IO₈

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Chemical Property of C₃₇H₄₃IO₈

Chemical Property:

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Technology Process of C₃₇H₄₃IO₈

There total 21 articles about C₃₇H₄₃IO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 482626-53-9
C₄₄H₅₀O₁₁S

: 374752-89-3
C₃₇H₄₃IO₈

Guidance literature:: With sodium iodide; In acetone; for 2h; Heating;
DOI:10.1021/ja016272z DOI:10.1021/ja0279646

Reference yield:

: 482626-35-7
(2R,3S,4S,5S)-5-Benzyloxymethoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-heptane-1,3-diol

: 374752-89-3
C₃₇H₄₃IO₈

Guidance literature:: Multi-step reaction with 14 steps

1: 100 percent / imidazole / CH₂Cl₂ / 1 h / 0 °C

2: 93 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

3: 93 percent / tetrabutylammonium fluoride / tetrahydrofuran / 8 h / 20 °C

4: 96 percent / triethylamine; sulfur trioxide pyridine complex / dimethylsulfoxide; CH₂Cl₂ / 3 h / 20 °C

5: 99 percent / MgBr₂*Et₂O / CH₂Cl₂ / 3 h / 20 °C

6: osmium tetroxide; NMO / acetone; H₂O / 1.5 h / 20 °C

7: NaIO₄ / acetone; H₂O / 0.5 h / 20 °C

8: 3.24 g / NaBH₄ / ethanol / 0.5 h / 20 °C

9: 93 percent / pyridine; DMAP / CH₂Cl₂ / 24 h / 20 °C

10: 88 percent / CAN / acetonitrile; H₂O / 0.5 h / 20 °C

11: 99 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

12: 99 percent / aq. HCl / acetonitrile / 2 h / 20 °C

13: 68 percent / p-TsOH*H₂O / CHCl₃ / 12 h / Heating

14: 99 percent / NaI / acetone / 2 h / Heating

With pyridine; 1H-imidazole; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; ammonium cerium(IV) nitrate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; triethylamine; sodium iodide; magnesium bromide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja0279646

Reference yield:

: 374752-81-5
(2S,3R,4R,5S)-3-Benzyloxy-5-benzyloxymethoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-heptanal

: 374752-89-3
C₃₇H₄₃IO₈

Guidance literature:: Multi-step reaction with 10 steps

1: 99 percent / MgBr₂*Et₂O / CH₂Cl₂ / 3 h / 20 °C

2: osmium tetroxide; NMO / acetone; H₂O / 1.5 h / 20 °C

3: NaIO₄ / acetone; H₂O / 0.5 h / 20 °C

4: 3.24 g / NaBH₄ / ethanol / 0.5 h / 20 °C

5: 93 percent / pyridine; DMAP / CH₂Cl₂ / 24 h / 20 °C

6: 88 percent / CAN / acetonitrile; H₂O / 0.5 h / 20 °C

7: 99 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

8: 99 percent / aq. HCl / acetonitrile / 2 h / 20 °C

9: 68 percent / p-TsOH*H₂O / CHCl₃ / 12 h / Heating

10: 99 percent / NaI / acetone / 2 h / Heating

With pyridine; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; ammonium cerium(IV) nitrate; toluene-4-sulfonic acid; triethylamine; sodium iodide; magnesium bromide; In ethanol; dichloromethane; chloroform; water; acetone; acetonitrile;
DOI:10.1021/ja0279646