N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Base Information

Chemical Name:N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol
CAS No.:1246635-34-6
Molecular Formula:C₄₀H₄₈N₄O₄
Molecular Weight:648.846
Hs Code.:

Synonyms:N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Suppliers and Price of N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

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Technology Process of N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

There total 6 articles about N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 69567-11-9,76738-52-8,126836-30-4
2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 6-azido-1-(4-methylbenzenesulfonate)hexan-1-ol

: 1246635-34-6
N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: With potassium carbonate; In acetonitrile; at 85 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c1ob05119a

Reference yield: 38.0%

: 69567-11-9,76738-52-8,126836-30-4
2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 235095-05-3
1-azido-6-bromohexane

: 1246635-34-6
N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: With dmap; triethylamine; In N,N-dimethyl-formamide; at 120 ℃; for 96h; Inert atmosphere;
DOI:10.1002/anie.201002802

Reference yield:

: 4286-55-9
1-bromo-6-hexanol

: 1246635-34-6
N-(6-azidohexyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / acetonitrile / 12 h / 85 °C / Inert atmosphere

With sodium azide; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c1ob05119a