1-azido-6-broMo-Hexane

Base Information

• Chemical Name: 1-azido-6-broMo-Hexane
• CAS No.: 235095-05-3
• Molecular Formula: C6H12BrN3
• Molecular Weight: 206.085
• Mol file: 235095-05-3.mol

Synonyms:6-azido-1-bromohexane;Hexane,1-azido-6-bromo;

Chemical Property of 1-azido-6-broMo-Hexane

Chemical Property:

• PSA: 49.75000
• LogP: 2.70476

Purity/Quality:

99% ^*data from raw suppliers

1-Azido-6-bromo-hexane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-azido-6-broMo-Hexane

There total 4 articles about 1-azido-6-broMo-Hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1 ,6-dibromohexane (629-03-8) → 1-azido-6-bromohexane (235095-05-3)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1002/bkcs.10134

Reference yield: 90.0%

6-Bromo-1-hexene (2695-47-8) → 1-azido-6-bromohexane (235095-05-3)

Guidance literature:

With 1-hydroxy-1,2-benzodioxol-3-(1H)-one; trimethylsilylazide; trifluoroacetic acid; In dichloromethane; water; at 0 - 22 ℃; Inert atmosphere;

DOI:10.1021/jacs.9b04381

Reference yield:

1-bromo-6-hexanol (4286-55-9) → 1-azido-6-bromohexane (235095-05-3)

Guidance literature:

With di-isopropyl azodicarboxylate; diphenylphosphoranyl azide; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 24h;

DOI:10.1039/c3tc31588f

upstream raw materials:

1 ,6-dibromohexane

1-bromo-6-hexanol

6-azidohexan-1-ol

6-Bromo-1-hexene

Downstream raw materials:

C₃₆H₇₃N₃O₆

C₄₂H₈₄N₆O₆

6-azidohexane-1-thiol

2,3,6-tri-O-benzyl-α-D-galactopyranosyl-(1->1)-2,3,4-tri-O-benzyl-6-O-(6-azidohexyl)-α-D-glucopyranoside