7-O-tosylneoclausenamide

Base Information

Chemical Name:7-O-tosylneoclausenamide
CAS No.:130202-81-2
Molecular Formula:C₂₅H₂₅NO₅S
Molecular Weight:451.543
Hs Code.:

Synonyms:7-O-tosylneoclausenamide

Suppliers and Price of 7-O-tosylneoclausenamide

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Chemical Property of 7-O-tosylneoclausenamide

Chemical Property:

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Technology Process of 7-O-tosylneoclausenamide

There total 9 articles about 7-O-tosylneoclausenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 130202-81-2
7-O-tosylneoclausenamide

Guidance literature:: Multi-step reaction with 8 steps

1: 57 percent / 4 Angstroem molecular sieve (activated), (+)-diethyl tartrate, titanium(IV)isopropoxide, tert-butyl hydroperoxide / CH₂Cl₂ / 48 h / -18 °C

2: 2,6-lutidine, sodium periodate, ruthenium(IV) oxide hydrate / acetonitrile; CCl₄; H₂O / 7 h

3: diethyl ether

4: 46 percent / sodium methoxide / methanol / 48 h / -18 °C

5: 81 percent / potassium permanganate, copper sulfate hydrate / CH₂Cl₂ / 3 h / Ambient temperature

6: 45 percent / tetramethylammonium hydroxide / CH₂Cl₂ / 5 h

7: 90 percent / pyridinium tosylate / CH₂Cl₂ / Ambient temperature

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; ruthenium(IV) oxide; potassium permanganate; sodium periodate; 4 A molecular sieve; tetramethyl ammoniumhydroxide; sodium methylate; pyridinium p-toluenesulfonate; copper(II) sulfate; (+)-Weinsaeure-diethylester; In methanol; tetrachloromethane; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1016/S0040-4020(01)85453-3

Reference yield:

: 68579-60-2,6589-55-5
2-(methylamino)-1-phenylethanol

: 130202-81-2
7-O-tosylneoclausenamide

Guidance literature:: Multi-step reaction with 5 steps

1: 46 percent / sodium methoxide / methanol / 48 h / -18 °C

2: 81 percent / potassium permanganate, copper sulfate hydrate / CH₂Cl₂ / 3 h / Ambient temperature

3: 45 percent / tetramethylammonium hydroxide / CH₂Cl₂ / 5 h

4: 90 percent / pyridinium tosylate / CH₂Cl₂ / Ambient temperature

With potassium permanganate; tetramethyl ammoniumhydroxide; sodium methylate; pyridinium p-toluenesulfonate; copper(II) sulfate; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)85453-3

Reference yield:

: 130202-79-8
(2R,3S)-2,3-Epoxy-N-methyl-N-phenacyl-3-phenylpropionamide

: 130202-81-2
7-O-tosylneoclausenamide

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / tetramethylammonium hydroxide / CH₂Cl₂ / 5 h

2: 90 percent / pyridinium tosylate / CH₂Cl₂ / Ambient temperature

With tetramethyl ammoniumhydroxide; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1016/S0040-4020(01)85453-3