N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

Base Information

Chemical Name:N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine
CAS No.:1256503-23-7
Molecular Formula:C₃₄H₄₁BrN₄O₈Si
Molecular Weight:741.711
Hs Code.:

N<sub>1</sub>-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

Synonyms:N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

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Technology Process of N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

There total 1 articles about N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 40510-88-1
1-acetoxy-2-chloromethoxyethane

: 1256503-22-6
5'-O-(tert-butyldiphenylsilyl)-2',3'-O-isopropylidene-8-bromoinosine

: 1256503-23-7
N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 1h; regioselective reaction;
DOI:10.1039/c0ob00090f

Reference yield: 59.0%

: 680-15-9
2,2-difluoro-2-(fluorosulfonyl)acetate

: 1256503-23-7
N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-bromoinosine

: 1256503-24-8
N₁-[(5''-acetoxyethoxy)methyl]-5'-O-TBDPS-2',3'-O-isopropylidene-8-tifluoromethylinosine

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; In N,N-dimethyl-formamide; at 70 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c0ob00090f