N₂,N₇-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide

Base Information

• Chemical Name: N₂,N₇-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide
• CAS No.: 1083159-46-9
• Molecular Formula: C₃₄H₄₆N₂O₆S₂
• Molecular Weight: 642.881

Synonyms:N₂,N₇-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide

Chemical Property of N₂,N₇-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide

Chemical Property:

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Technology Process of N₂,N₇-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide

There total 1 articles about N₂,N₇-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-tert-butylcyclohexylamine (5400-88-4) + 9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonyl dichloride (36003-56-2) → N2,N7-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide (1083159-46-9)

Guidance literature:

With triethylamine; In dichloromethane; at -50 - 20 ℃;

Reference yield: 53.0%

N2,N7-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide (1083159-46-9) + 3-(dimethylamino)propyl chloride hydrochloride (5407-04-5) → N2,N7-bis(4-tert-butylcyclohexyl)-N2-(3-(dimethylamino)propyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide (1083163-27-2) + N2,N7-bis(4-tert-butylcyclohexyl)-N2,N7-bis(3-(dimethylamino)propyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide (1215126-86-5)

Guidance literature:

N₂,N₇-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide; With sodium hydride; In N,N-dimethyl-formamide; for 0.0833333h; Inert atmosphere; Cooling with ice;

3-(dimethylamino)propyl chloride hydrochloride; In N,N-dimethyl-formamide; at 40 ℃; for 72.24h; Inert atmosphere; Cooling with ice;

Reference yield:

N2,N7-bis(4-tert-butylcyclohexyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide (1083159-46-9) → N2,N7-bis(4-tert-butylcyclohexyl)-N2-(3-(dimethylamino)propyl)-9,10-bis(hydroxyimino)-9,10-dihydroanthracene-2,7-disulfonamide hydrochloride

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / Inert atmosphere; Cooling with ice

1.2: 72 h / 40 °C

2.1: pyridine; hydroxylamine hydrochloride / 36 h / 95 °C

With pyridine; hydroxylamine hydrochloride; sodium hydride; In N,N-dimethyl-formamide;

upstream raw materials:

4-tert-butylcyclohexylamine

9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonyl dichloride

Downstream raw materials:

N₂,N₇-bis(4-tert-butylcyclohexyl)-N₂-(3-(dimethylamino)propyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide

N₂,N₇-bis(4-tert-butylcyclohexyl)-N₂,N₇-bis(3-(dimethylamino)propyl)-9,10-dioxo-9,10-dihydroanthracene-2,7-disulfonamide

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