2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester

Base Information

• Chemical Name: 2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester
• CAS No.: 1236198-60-9
• Molecular Formula: C₄₆H₅₄N₄O₁₀
• Molecular Weight: 822.956

Synonyms:2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester

Chemical Property of 2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester

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Technology Process of 2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester

There total 1 articles about 2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

benzyl N-(tert-butoxycarbonyl)-O-(prop-2-yn-1-yl)-L-serinate (1190744-99-0) + 1-methyl-6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranoside (220129-77-1) → 2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester (1236198-60-9)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 12h;

DOI:10.5012/bkcs.2010.31.04.1055

Reference yield: 93.0%

2-(tert-butoxycarbonylamino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoate benzyl ester (1236198-60-9) → (S)-2-((tert-butoxycarbonyl)amino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoic acid (1316262-44-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; for 0.333333h;

DOI:10.1016/j.bmc.2011.05.049

upstream raw materials:

benzyl N-(tert-butoxycarbonyl)-O-(prop-2-yn-1-yl)-L-serinate

1-methyl-6-azido-2,3,4-tri-O-benzyl-6-deoxy-α-D-mannopyranoside

Downstream raw materials:

(S)-2-((tert-butoxycarbonyl)amino)-3-((1-(((2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-6-methoxytetrahydro-2H-pyran-2-yl)methyl)-1H-1,2,3-triazol-4-yl)methoxy)propanoic acid

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