p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

Base Information

Chemical Name:p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside
CAS No.:127086-70-8
Molecular Formula:C₂₅H₂₀N₂O₈
Molecular Weight:476.442
Hs Code.:

Synonyms:p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

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Chemical Property of p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

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Technology Process of p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

There total 4 articles about p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 127179-71-9
p-nitrophenyl endo-2',3'-O-(1-methoxycarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

: 127086-70-8
p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

Guidance literature:: With ammonia; In ethanol; at -70 - 90 ℃;

Reference yield:

: 1573-92-8
9-oxo-9H-fluorene-1-carboxylic acid

: 127086-70-8
p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) p-toluenesulfonic acid / 1.) reflux, 2.) reflux, overnight

2: 25 percent / pyridinium tosylate / 1,2-dichloro-ethane / 1.) from RT to 55 deg C, 4 h, 2.) 55 deg C, 48 h

3: 5 percent / NH₃ / ethanol / -70 - 90 °C

With ammonia; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In ethanol; 1,2-dichloro-ethane;

Reference yield:

: 116910-84-0
9,9-dimethoxy-1-methoxycarbonylfluorene

: 127086-70-8
p-nitrophenyl endo-2',3'-O-(1-aminocarbonyl-o,o'-biphenylenemethylidene)ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 25 percent / pyridinium tosylate / 1,2-dichloro-ethane / 1.) from RT to 55 deg C, 4 h, 2.) 55 deg C, 48 h

2: 5 percent / NH₃ / ethanol / -70 - 90 °C

With ammonia; pyridinium p-toluenesulfonate; In ethanol; 1,2-dichloro-ethane;