pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

Base Information

Chemical Name:pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate
CAS No.:83089-86-5
Molecular Formula:C₂₀H₂₁Cl₅N₂O₄
Molecular Weight:530.663
Hs Code.:

Synonyms:pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

Suppliers and Price of pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

There total 6 articles about pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 87-86-5,67471-28-7
Pentachlorophenol

: 4-(2-tert-Butoxycarbonylamino-ethyl)-3,5-dimethyl-1H-pyrrole-2-carboxylic acid

: 83089-86-5
pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 40h;

Reference yield:

: 20303-31-5
benzyl 4-(2-methoxycarbonylethyl)-3,5-dimethylpyrrole-2-carboxylate

: 83089-86-5
pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / hydrazine hydrate / ethanol / 3 h / Heating

2: aq. HCl, NaNO₂ / H₂O / 0.5 h / 0 °C

3: benzene / 2 h / Heating

4: 63 percent / trifluoroacetic acid / benzene / 4 h / Heating

5: triethylamine, H₂ / Pd/C / tetrahydrofuran / 2 h

6: 73 percent / dicyclohexylcarbodi-imide / CH₂Cl₂ / 40 h / 0 °C

With hydrogenchloride; hydrogen; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water; benzene;

Reference yield:

: 28844-01-1
benzyl 4-(2-hydrazidoethyl)-3,5-dimethylpyrrole-2-carboxylate

: 83089-86-5
pentachlorophenyl 3,5-dimethyl-4-(2-t-butoxycarbonylaminoethyl)pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: aq. HCl, NaNO₂ / H₂O / 0.5 h / 0 °C

2: benzene / 2 h / Heating

3: 63 percent / trifluoroacetic acid / benzene / 4 h / Heating

4: triethylamine, H₂ / Pd/C / tetrahydrofuran / 2 h

5: 73 percent / dicyclohexylcarbodi-imide / CH₂Cl₂ / 40 h / 0 °C

With hydrogenchloride; hydrogen; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; benzene;