Technology Process of Boc-LeuΨCha-OBzl
There total 5 articles about Boc-LeuΨCha-OBzl which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride; acetic acid;
In
ethanol;
for 2h;
Heating;
DOI:10.1021/jm00047a020
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) 2 M aq. KHSO4, 2.) 4-(dimethylamino)pyridine, N,N'-dicyclohexylcarobodiimide / 1.) ethyl acetate, 2.) CH2Cl2, a) 0 deg C, 10 min, b) RT, 2 h
2: 43 percent / NaBH3CN, CH3COOH / methanol / 1 h / 0 °C
3: 26 percent / 1percent CH3COOH, NaBH3CN / ethanol / 2 h / Heating
With
dmap; potassium hydrogensulfate; sodium cyanoborohydride; acetic acid; dicyclohexyl-carbodiimide;
In
methanol; ethanol;
DOI:10.1021/jm00047a020
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 43 percent / NaBH3CN, CH3COOH / methanol / 1 h / 0 °C
2: 26 percent / 1percent CH3COOH, NaBH3CN / ethanol / 2 h / Heating
With
sodium cyanoborohydride; acetic acid;
In
methanol; ethanol;
DOI:10.1021/jm00047a020
