BOC-CHA-OH DCHA

Base Information

• Chemical Name: BOC-CHA-OH DCHA
• CAS No.: 37462-62-7
• Molecular Formula: C26H48N2O4
• Molecular Weight: 452.67
• Hs Code.: 2924 29 70
• Mol file: 37462-62-7.mol

Synonyms:T-BUTOXYCARBONYL-BETA-CYCLOHEXYL-L-ALANINE DICYCLOHEXYLAMINE SALT DCHA;T-BUTOXYCARBONYL-3-HEXAHYDRO-L-PHENYLALANINE DCHA;N-ALPHA-T-BOC-BETA-CYCLOHEXYL-L-ALANINE DICYCLOHEXYLAMMONIUM SALT;BOC-3-CYCLOHEXYL-L-ALANINE DICYCLOHEXYLAMINE SALT;BOC-3-CYCLOHEXYL-L-ALANINE DICYCLOHEXYLAMMONIUM SALT;BOC-BETA-CYCLOHEXYL-L-ALANINE DICYCLOHEXYLAMMONIUM SALT;BOC-CHA-OH DCHA;BOC-L-3-CYCLOHEXYL-L-ALANINE DICYCLOHEXYLAMINE SALT

Chemical Property of BOC-CHA-OH DCHA

Chemical Property:

• PSA: 87.66000
• LogP: 6.95790
• Storage Temp.: Store at RT.

Purity/Quality:

97% ^*data from raw suppliers

Boc-Cha-OH . DCHA 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BOC-CHA-OH DCHA

There total 1 articles about BOC-CHA-OH DCHA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) + cyclohexylamine (108-91-8,157973-60-9) → Boc-Cha-OH * dicyclohexylamine (37462-62-7)

Guidance literature:

In diethyl ether; ethanol; rhodium; ethyl acetate;

Reference yield:

Boc-Cha-OH * dicyclohexylamine (37462-62-7) → Boc-LeuΨCha-OH

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) 2 M aq. KHSO₄, 2.) 4-(dimethylamino)pyridine, N,N'-dicyclohexylcarobodiimide / 1.) ethyl acetate, 2.) CH₂Cl₂, a) 0 deg C, 10 min, b) RT, 2 h

2: 43 percent / NaBH₃CN, CH₃COOH / methanol / 1 h / 0 °C

3: 26 percent / 1percent CH₃COOH, NaBH₃CN / ethanol / 2 h / Heating

4: 99 percent / H₂ / 10percent Pd/C / aq. ethanol / 2 h

With dmap; potassium hydrogensulfate; hydrogen; sodium cyanoborohydride; acetic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol;

DOI:10.1021/jm00047a020

Reference yield:

Boc-Cha-OH * dicyclohexylamine (37462-62-7) → Boc-LeuΨCha-OBzl (160908-85-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) 2 M aq. KHSO₄, 2.) 4-(dimethylamino)pyridine, N,N'-dicyclohexylcarobodiimide / 1.) ethyl acetate, 2.) CH₂Cl₂, a) 0 deg C, 10 min, b) RT, 2 h

2: 43 percent / NaBH₃CN, CH₃COOH / methanol / 1 h / 0 °C

With dmap; potassium hydrogensulfate; sodium cyanoborohydride; acetic acid; dicyclohexyl-carbodiimide; In methanol;

DOI:10.1021/jm00047a020

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine

cyclohexylamine

Downstream raw materials:

Boc-Cha-D-Glu(Bzl)-OBzl

Boc-Cha-OBzl

Boc-LeuΨCha-OBzl

Boc-LeuΨCha-OBzl

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