2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

Base Information

Chemical Name:2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine
CAS No.:1418128-59-2
Molecular Formula:C₂₉H₃₈BNO₃Si
Molecular Weight:487.522
Hs Code.:

Synonyms:2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

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Chemical Property of 2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

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Technology Process of 2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

There total 4 articles about 2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1418128-56-9
2-[2-(tert-butyl-diphenyl-silanyloxymethyl)-3-nitro-phenyl]-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1418128-59-2
2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 20h; under 760.051 Torr;

Reference yield:

: 861106-91-4
(2-bromo-6-nitro-phenyl)-methanol

: 1418128-59-2
2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 - 50 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 4 h / 90 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 h / 20 °C / 760.05 Torr

With 1H-imidazole; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; hydrogen; potassium acetate; In 1,4-dioxane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1418128-54-7
(2-bromo-6-nitro-benzyloxy)-tert-butyl-diphenyl-silane

: 1418128-59-2
2-(tert-butyl-diphenyl-silanyloxymethyl)-3-(4,4,5,5-tetramethyl-[1,3,2]dioxborolan-2-yl)-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 4 h / 90 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 h / 20 °C / 760.05 Torr

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; hydrogen; potassium acetate; In 1,4-dioxane; ethyl acetate;